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RAS PhysicsПоверхность. Рентгеновские, синхротронные и нейтронные исследования Journal of Surface Investigation. X-Ray, Synchrotron and Neutron Techniques

  • ISSN (Print) 1028-0960
  • ISSN (Online) 3034-5731

Photocatalytic Activity of Ba-Doped BiFeO Nanoparticles

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PII
S30345731S1028096025040138-1
DOI
10.7868/S3034573125040138
Publication type
Article
Status
Published
Authors
R. R. Gyulakhmedov
  • Affiliation: Dagestan State University
F. F. Orudzhev
  • Affiliation:
    Dagestan State University
    Institute of Physics, Dagestan Federal Research Center of the Russian Academy of Sciences
A. N. Khrustalev
  • Affiliation: MIREA - Russian Technological University
D. S. Sobola
  • Affiliation: Brno Technical University
M. G. Abdurakhmanov
  • Affiliation: Dagestan State University
Sh. P. Faradzhev
  • Affiliation: Dagestan State University
A. E. Muslimov
  • Affiliation: A.V. Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the National Research Centre “Kurchatov Institute”
V. M. Kanevsky
  • Affiliation: A.V. Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the National Research Centre “Kurchatov Institute”
M. Kh. Rabadanov
  • Affiliation: Dagestan State University
N.-M. R. Alikhanov
  • Affiliation:
    Dagestan State University
    Institute of Physics, Dagestan Federal Research Center of the Russian Academy of Sciences
Volume/ Edition
Volume / Issue number 4
Pages
89-100
Abstract
In this work, nanopowders of the BiBaFeO system (x=0, 0.10, 0.20) were synthesized by the combustion method of nitrate-organic precursors. The effect of doping bismuth ferrite (BiFeO) with barium (Ba) ions on the morphology, crystal structure and photocatalytic activity of the material was studied. X-ray diffraction analysis showed that all samples crystallize into a rhombohedrally distorted perovskite structure with the R3c space group. Doping with barium led to a significant decrease in the crystallite sizes, as well as to a distortion of the crystal lattice. In the case of 20% substitution, the formation of BaCO impurity was observed, which was also confirmed by the analysis of the Raman spectra. It is shown that the introduction of barium leads to the formation of a more porous texture and a significant increase in the specific surface area of the material. The original BiFeO demonstrated an extremely low efficiency of methylene blue decomposition relative to photolysis, while doping with barium led to a significant improvement in the photocatalytic characteristics of the material: in the case of 20% Ba substitution, the decomposition of methylene blue reached 99% in 1 hour.
Keywords
феррит висмута BiFeO3 барий синтез легирование нанопорошок фотокатализ метиленовый синий структура комбинационное рассеяние света
Date of publication
20.01.2025
Year of publication
2025
Number of purchasers
0
Views
58

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